| 1. |
- Manchili, Swathi Kiranmayee, 1987, et al.
(författare)
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Surface analysis of iron and steel nanopowder
- 2018
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Ingår i: Surface and Interface Analysis. - : Wiley. - 1096-9918 .- 0142-2421. ; 50:11, s. 1083-1088-10886
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Tidskriftsartikel (refereegranskat)abstract
- High sinter density is desired in powder metallurgy components as the requirement for performance is increasing day‐by‐day. One of the promising ways to achieve improved densification during sintering is through the addition of nanopowder to the conventional micrometer sized metal powder. It is well known that the surface chemistry of the powder has a decisive effect on sintering and consequently the properties of the components produced. Extensive research has hence been conducted to elucidate the surface chemistry and its influence on sintering for powder used in conventional powder metallurgy. Nanopowder, owing to high surface to volume ratio, can contribute to the activation of sintering at lower temperatures and enhance the sinter density. In this context, the surface chemistry of the nanopowder is also expected to exhibit substantial influence on sintering. The present investigation is aimed at establishing a methodology to study the surface chemistry and oxide thickness of nanopowder. For this purpose, iron nanopowder of 3 different size fractions: 35 to 45, 40 to 60, and 60 to 80 nm with core‐shell structure were studied. Different approaches were adopted to evaluate the shell thickness of the iron nanoparticles. The methodology was developed and tried on low alloy steel nanopowder to measure oxide thickness. X‐ray photoelectron spectroscopy, thermogravimetry, and high‐resolution scanning electron microscopy techniques were used to study the nanopowder. Results from different core‐shell models for iron nanopowder were found to be consistent except in the case where depth profiling was taken into account. The results were in agreement with the values obtained from thermogavimetry‐surface area correlation.
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| 2. |
- Jeong, Seung Hee, 1978-, et al.
(författare)
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Stretchable Thermoelectric Generators Metallized with Liquid Alloy
- 2017
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Ingår i: ACS Applied Materials & Interfaces. - : American Chemical Society (ACS). - 1944-8252 .- 1944-8244. ; 9:18, s. 15791-15797
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Tidskriftsartikel (refereegranskat)abstract
- Conventional thermoelectric generators (TEGs) are normally hard, rigid, and flat. However, most objects have curvy surfaces, which require soft and even stretchable TEGs for maximizing efficiency of thermal energy harvesting. Here, soft and stretchable TEGs using conventional rigid Bi2Te3 pellets metallized with a liquid alloy is reported. The fabrication is implemented by means of a tailored layer-by-layer fabrication process. The STEGs exhibit an output power density of 40.6 ?W/cm2 at room temperature. The STEGs are operational after being mechanically stretched-and-released more than 1000 times, thanks to the compliant contact between the liquid alloy interconnects and the rigid pellets. The demonstrated interconnect scheme will provide a new route to the development of soft and stretchable energy-harvesting avenues for a variety of emerging electronic applications.
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| 3. |
- Kabiri Samani, Majid, 1976, et al.
(författare)
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Improving Thermal Transport at Carbon Hybrid Interfaces by Covalent Bonds
- 2018
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Ingår i: Advanced Materials Interfaces. - : Wiley. - 2196-7350. ; 2018:5
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Tidskriftsartikel (refereegranskat)abstract
- Graphene and carbon nanotubes have received much attention for thermal management application due to their unique thermal performance. Theoretical work suggests that a covalent bond can combine 1D carbon nanotubes with 2D graphene together to extend the excellent thermal property to three dimensions for heat dissipation. This paper experimentally demonstrates the high heat dissipation capability of a freestanding 3D multiwall carbon nanotube (MWCNT) and graphene hybrid material. Using high-resolution transmission electron microscopy and pulsed photothermal reflection measurement method, the covalent bonds between MWCNT and planar graphene are microscopically and numerically demonstrated. Thermal resistance at the junction with covalent bonds is 9×10^−10 Kelvin square meter per watt, which is three orders of magnitude lower than van der Waals contact. Joule heating method is used to verify the extra cooling effect of this 3D hybrid material compared to graphite film. A demonstrator using high power chip is developed to demonstrate the applicability of this hybrid material in thermal application. Temperature at hot spots can be decreased by around 10°C with the assistance of this hybrid material. These findings are very significant for understanding the thermal conduction during combining 1D and 2D carbon material together for future thermal management application.
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| 4. |
- Jeong, Seung Hee, et al.
(författare)
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Mechanically Stretchable and Electrically Insulating Thermal Elastomer Composite by Liquid Alloy Droplet Embedment
- 2015
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Ingår i: Scientific Reports. - : Springer Science and Business Media LLC. - 2045-2322. ; 5
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Tidskriftsartikel (refereegranskat)abstract
- Stretchable electronics and soft robotics have shown unsurpassed features, inheriting remarkable functions from stretchable and soft materials. Electrically conductive and mechanically stretchable materials based on composites have been widely studied for stretchable electronics as electrical conductors using various combinations of materials. However, thermally tunable and stretchable materials, which have high potential in soft and stretchable thermal devices as interface or packaging materials, have not been sufficiently studied. Here, a mechanically stretchable and electrically insulating thermal elastomer composite is demonstrated, which can be easily processed for device fabrication. A liquid alloy is embedded as liquid droplet fillers in an elastomer matrix to achieve softness and stretchability. This new elastomer composite is expected useful to enhance thermal response or efficiency of soft and stretchable thermal devices or systems. The thermal elastomer composites demonstrate advantages such as thermal interface and packaging layers with thermal shrink films in transient and steady-state cases and a stretchable temperature sensor.
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| 5. |
- Lv, Zhen, et al.
(författare)
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Highly thermally conductive substrate based on graphene film
- 2021
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Ingår i: 2021 23rd European Microelectronics and Packaging Conference and Exhibition, EMPC 2021. ; , s. 195-199
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Konferensbidrag (refereegranskat)abstract
- Heat dissipation has become one of the critical challenges of development for microelectronic products because of the increasing of heat accumulation in the devices. A novel laminated composite with high thermal conductivity was fabricated by hot-pressing using graphene films (GFs) and glass fiber reinforced epoxy resin (GFEP). The effect of GFs with different thicknesses and number of layers on the thermal properties of the composites was investigated. An in-plane thermal conductivity of 141 W · m-1 · K-1 for the laminated composites with GFs and GFEP were obtained. The heat dissipation capability of GFs/GFEP composites is evaluated by infrared thermal imaging technology. The maximum temperature difference between the heating elements on GFs/GFEP composites and GFEP increases with the rise of voltage applied to the heating elements. Moreover, the heat dissipation capability of the composite is enhanced with the increased of the number of layers of GFs. The temperature of the heating element assembled on GFs/GFEP composites is 144.3°C lower than that on GFEP at the same voltage. The results indicate that the GFs/GFEP composites is a promising candidate of substrate material with high heat dissipation capability.
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| 6. |
- Enmark, Markus, 1991, et al.
(författare)
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Reliability Characterization of Graphene Enhanced Thermal Interface Material for Electronics Cooling Applications
- 2022
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Ingår i: 2022 IMAPS Nordic Conference on Microelectronics Packaging, NordPac 2022.
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Konferensbidrag (refereegranskat)abstract
- Graphene-based products are gaining popularity in thermal management applications in high performance electronics systems. The ultra-high thermal conductivity of graphene together with its relatively low density makes it a suitable material for reaching high cooling capability in lightweight applications. An example of products that are starting to enter the market is graphene enhanced thermal interface materials (TIMs). Pristine graphene enhanced TIMs are well characterized and show high thermal conductivity and low thermal interface resistance. Before these TIMs can take the next step from being a niche product to reach high volume sales on the market, it needs to be proven that they have stable performance over time when conditioned and aged according to industry reliability standards. In this work, a set of customized test rigs was designed, and graphene enhanced TIMs of three different thicknesses were tested. The TIMs were compressed by 30% and then subjected to three different industry standard reliability tests; thermal aging, temperature cycling and damp heat. The thermal resistance was measured sequentially during each test to monitor change over time. The reliability tests are still ongoing and so far the tested graphene enhanced TIMs have stable performance over time with some observable trends for the different tests. At the current test time the maximum degradation in thermal resistance is 13%, measured after 511 cycles in the thermal cycling test. The used test method is deemed promising for reliability comparison and future requirement standardization on thermal pads.
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| 7. |
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| 8. |
- Banerjee, Debashree, et al.
(författare)
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Elevated thermoelectric figure of merit of n-type amorphous silicon by efficient electrical doping process
- 2018
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Ingår i: Nano Energy. - : Elsevier BV. - 2211-2855 .- 2211-3282. ; 44, s. 89-94
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Tidskriftsartikel (refereegranskat)abstract
- The currently dominant thermoelectric (TE) materials used in low to medium temperature range contain Tellurium that is rare and mild-toxic. Silicon is earth abundant and environment friendly, but it is characterized by a poor TE efficiency with a low figure of merit, ZT. In this work, we report that ZT of amorphous silicon (a-Si) thin films can be enhanced by 7 orders of magnitude, reaching ∼0.64 ± 0.13 at room temperature, by means of arsenic ion implantation followed by low-temperature dopant activation. The dopant introduction employed represents a highly controllable doping technique used in standard silicon technology. It is found that the significant enhancement of ZT achieved is primarily due to a significant improvement of electrical conductivity by doping without crystallization so as to maintain the thermal conductivity and Seebeck coefficient at the level determined by the amorphous state of the silicon films. Our results open up a new route towards enabling a-Si as a prominent TE material for cost-efficient and environment-friendly TE applications at room temperature.
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| 9. |
- Bao, Jie, et al.
(författare)
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Synthesis and Applications of Two-Dimensional Hexagonal Boron Nitride in Electronics Manufacturing
- 2016
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Ingår i: Electronic Materials Letters. - : Springer Science and Business Media LLC. - 1738-8090 .- 2093-6788. ; 12:1, s. 1-16
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Forskningsöversikt (refereegranskat)abstract
- In similarity to graphene, two-dimensional (2D) hexagonal boron nitride (hBN) has some remarkable properties, such as mechanical robustness and high thermal conductivity. In addition, hBN has superb chemical stability and it is electrically insulating. 2D hBN has been considered a promising material for many applications in electronics, including 2D hBN based substrates, gate dielectrics for graphene transistors and interconnects, and electronic packaging insulators. This paper reviews the synthesis, transfer and fabrication of 2D hBN films, hBN based composites and hBN-based van der Waals heterostructures. In particular, this review focuses on applications in manufacturing electronic devices where the insulating and thermal properties of hBN can potentially be exploited. 2D hBN and related composite systems are emerging as new and industrially important materials, which could address many challenges in future complex electronics devices and systems.
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| 10. |
- Casa, Marcello, et al.
(författare)
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Silver decorated graphene-polyvinyl alcohol hybrid hydrogel as catalyst for benzonitrile conversion
- 2017
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Ingår i: Advanced Science Letters. - : American Scientific Publishers. - 1936-7317 .- 1936-6612. ; 23:6, s. 5980-5983
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Tidskriftsartikel (refereegranskat)abstract
- In this work, we have synthetized a reduced graphene oxide functionalized with silver nanoparticles (G/Ag) by a method developed in our previous study and incorporated it in a hydrogel based on polyvinyl alcohol (PVA) as gelator through a freezing/thawing method. The hydrogel has been tested to catalyze the reduction at room temperature of nitrile group of benzonitrile in water by using glucose as a natural and mild reducing agent.
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